Rapid sol gel synthesis of BaFe12O19 nanoparticles: An excellent catalytic application in the electrochemical detection of tramadol in the presence of acetaminophen

Published on Jul 1, 2020in Microchemical Journal3.594
· DOI :10.1016/J.MICROC.2020.104803
Zoheira Bagherinasab1
Estimated H-index: 1
(IAU: Islamic Azad University),
Hadi Beitollahi66
Estimated H-index: 66
(Graduate University of Advanced Technology)
+ 2 AuthorsMalak Hekmati13
Estimated H-index: 13
(IAU: Islamic Azad University)
Abstract The present study reports synthesis of BaFe12O19 nanoparticles by sol gel technique followed by its characterization using Energy dispersive X-ray spectroscopy (EDS), X-Ray diffraction (XRD), field emission scanning electron microscopy (FESEM), vibrating sample magnetometer (VSM) analysis, and Fourier-transform infrared spectroscopy (FTIR). The BaFe12O19 nanoparticles have been applied to construct a modified graphite screen-printed electrode (GSPE). BaFe12O19/GSPE has been applied as a working electrode in the analysis of tramadol and acetaminophen by voltammetric techniques. The BaFe12O19/GSPE showed a good selectiveness for analysis of tramadol in the presence of acetaminophen with the separated peak potentials at ∼ 230 mV, and ∼ 700 mV, respectively. Excellent linear calibration curves, ranging from 0.08 to 500.0 µM for tramadol and from 5.0 to 500.0 µM for acetaminophen, with detection limits of 0.025 and 1.5 µM were obtained.
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