Original paper
Synthesis of an NHC-Coordinated Dialkyldisilavinylidene and Its Oxidation Providing a Silicon Analog of an Acetolactone
Abstract
Although isolable silicon analogs of acetylene have been extensively studied, the silicon analogs of vinylidene, which is a short-lived isomer of acetylene, remain scarce. Herein, we report isolable NHC-coordinated dialkyldisilavinylidene 1 synthesized by the reduction of a tetrabromodisilane featuring a bulky alkyl protecting group. 1 was fully characterized by a combination of multinuclear NMR spectroscopy, high-resolution mass spectrometry,...
Paper Details
Title
Synthesis of an NHC-Coordinated Dialkyldisilavinylidene and Its Oxidation Providing a Silicon Analog of an Acetolactone
Published Date
Apr 1, 2021
Journal
Volume
40
Issue
7
Pages
843 - 847
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Notes
History