HILIC characterization: Estimation of phase volumes and composition for a zwitterionic column
Abstract
A methodology for the estimation of the different phase volumes in HILIC is presented. For a ZIC-HILIC column the mobile phase volume (hold-up volume) is determined in several acetonitrile- and methanol-water compositions by a Linear Free Energy Relationships (LFER) homologous series approach involving n-alkyl-benzenes, -phenones, and -ketones. We demonstrate that the column works as a HILIC column when the mobile phase contains high and medium...
Paper Details
Title
HILIC characterization: Estimation of phase volumes and composition for a zwitterionic column
Published Date
Sep 1, 2020
Journal
Volume
1130
Pages
39 - 48
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