Simultaneous enantioselective determination of 22 chiral pesticides in fruits and vegetables using chiral liquid chromatography coupled with tandem mass spectrometry

This paper presents a novel multi-residue method for the enantioselective analysis of 22 chiral pesticides in cucumber, tomato, cabbage, grape, mulberry, apple and pear at enantiomeric levels. Pesticides were efficiently extracted by magnetic solid-phase extraction based on graphene as sorbent. Response surface methodology was used to assist the multivariable optimization. The perfect chiral separation of the enantiomers was achieved on a...