STUDY ON SYNTHESIS OF 4-METHYL-4′-AMINODIBENZENE ETHER WITH THIOUREA DIOXIDE
Abstract
With 4 methyl 4′ nitrodibenzene ether,thiourea dioxide and sodium hydroxide as starting materials,the 4 methyl 4′ aminodibenzene ether is synthesized in aqueous ethanolic solution.The optimum conditions of the reaction are as follows∶4 melthyl 4′ nitrodibenzene ether∶thiourea dioxide∶sodium hydroxide is 1.0mol∶3.9mol∶7.5mol,the duration of additron of thiourea dioxide for the present scale is 1.0h,suitable temperature is 50℃,reaction time is...
Paper Details
Title
STUDY ON SYNTHESIS OF 4-METHYL-4′-AMINODIBENZENE ETHER WITH THIOUREA DIOXIDE
Published Date
Jan 1, 2000
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