Conversion to isothiocyanates via dithiocarbamates for the determination of aromatic primary amines by headspace-solid phase microextraction and gas chromatography
Abstract
A novel and highly selective method has been developed for the determination of aromatic primary amines by their conversion to dithiocarbamates by reaction with carbon disulphide, and then to isothiocyanates, which are volatile, by heating in the presence of a heavy metal ion. Zinc(II) was selected owing to its low toxicity and optimum yield of isothiocyanates. The latter were sampled by headspace-solid phase microextraction (HS-SPME) on...
Paper Details
Title
Conversion to isothiocyanates via dithiocarbamates for the determination of aromatic primary amines by headspace-solid phase microextraction and gas chromatography
Published Date
Nov 1, 2013
Journal
Volume
801
Pages
48 - 58
Citation AnalysisPro
You’ll need to upgrade your plan to Pro
Looking to understand the true influence of a researcher’s work across journals & affiliations?
- Scinapse’s Top 10 Citation Journals & Affiliations graph reveals the quality and authenticity of citations received by a paper.
- Discover whether citations have been inflated due to self-citations, or if citations include institutional bias.
Notes
History