Headspace in-drop derivatization of carbonyl compounds for their analysis by high-performance liquid chromatography-diode array detection
Abstract
A simple and rapid method has been reported for the determination of carbonyl compounds involving sample preparation by headspace single drop microextraction using 1-butanol as extraction solvent containing 2,4-dinitrophenylhydrazine for hydrazone formation, and direct transfer of the drop into the injector for high-performance liquid chromatography with diode array detection. An angle-cut polytetrafluoroethylene sleeve, 3 mm × 0.5 mm, was fixed...
Paper Details
Title
Headspace in-drop derivatization of carbonyl compounds for their analysis by high-performance liquid chromatography-diode array detection
Published Date
Jan 1, 2009
Journal
Volume
632
Issue
2
Pages
208 - 215
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