Research on Additives Assisted Catalytic Cyclo-Dehydration of 1, 4-Butanediol to Tetrahydrofuran in Near-Critical Water
Abstract
We herein report the cyclo-dehydration of 1,4-butanediol (BD) assisted with additives to form tetrahydrofuran (THF) in near-critical water (NCW).Three additives including Fe2(SO4)3,ZnSO4 and NaHSO4 were screened. Effects of various experimental parameters such as temperature (260-340°C), time (60-180min), reactant/water ratio (r/w, 1:10-1:40) and pressure (15-25MPa) on the yield of THF were examined. Without the presence of additives, the...
Paper Details
Title
Research on Additives Assisted Catalytic Cyclo-Dehydration of 1, 4-Butanediol to Tetrahydrofuran in Near-Critical Water
Published Date
Jul 1, 2012
Journal
Volume
550-553
Pages
693 - 698
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